Cover for Gas Chromatography with Glass Capillary Columns

Gas Chromatography with Glass Capillary Columns

Book1978

Authors:

WALTER JENNINGS

Gas Chromatography with Glass Capillary Columns

Book1978

 

Cover for Gas Chromatography with Glass Capillary Columns

Authors:

WALTER JENNINGS

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Book description

Gas Chromatography with Glass Capillary Columns describes glass capillary technology and the selection, installation, evaluation, and use of glass open tubular columns for gas chro ... read full description

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  2. Book chapterNo access

    CHAPTER 1 - INTRODUCTION

    Pages 1-18

  3. Book chapterNo access

    CHAPTER 2 - THE GLASS CAPILLARY COLUMN

    Pages 19-29

  4. Book chapterNo access

    CHAPTER 3 - COLUMN COATING

    Pages 31-42

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    CHAPTER 4 - Inlet Systems

    Pages 43-54

  6. Book chapterNo access

    CHAPTER 5 - COLUMN INSTALLATION

    Pages 55-66

  7. Book chapterNo access

    CHAPTER 6 - MEASURING COLUMN EFFICIENCY

    Pages 67-74

  8. Book chapterNo access

    CHAPTER 7 - TREATMENT OF RETENTION DATA

    Pages 75-82

  9. Book chapterNo access

    CHAPTER 8 - TEMPERATURE PROGRAMMING AND CARRIER FLOW CONSIDERATIONS

    Pages 83-91

  10. Book chapterNo access

    CHAPTER 9 - COLUMN STABILITY

    Pages 93-98

  11. Book chapterNo access

    CHAPTER 10 - COLUMN SELECTION

    Pages 99-104

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    CHAPTER 11 - SAMPLE PREPARATION

    Pages 105-118

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    CHAPTER 12 - ANALYSIS OF MATERIALS OF RESTRICTED VOLATILITY

    Pages 119-122

  14. Book chapterNo access

    CHAPTER 13 - APPLICATIONS OF GLASS CAPILLARY GAS CHROMATOGRAPHY

    Pages 123-146

  15. Book chapterNo access

    APPENDIX I - NOMENCLATURE

    Pages 147-152

  16. Book chapterNo access

    APPENDIX II - LIQUID PHASES

    Pages 153-158

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    APPENDIX III - POROUS POLYMER DATA

    Pages 159-171

  18. Book chapterNo access

    APPENDIX IV - SILYLATION AND DERIVATIZATION REACTIONS

    Pages 173-179

  19. Book chapterNo access

    INDEX

    Pages 181-184

About the book

Description

Gas Chromatography with Glass Capillary Columns describes glass capillary technology and the selection, installation, evaluation, and use of glass open tubular columns for gas chromatography. Discussions are organized around the glass capillary column; column coating and installation; inlet systems; measurement of column efficiency; temperature programming and carrier flow; and retention behavior. Column selection and stability and sample preparation are also covered. This text is comprised of 13 chapters; the first of which introduces the reader to the practical considerations involved in the selection, installation, evaluation, and use of high-resolution open tubular glass capillary columns, along with the theory of the chromatographic process. The discussion then turns to the influence of operating parameters and storage conditions on the interrelated forces involved in coating glass capillary columns; the dynamic and static techniques of column coating; and design defects in the inlet system caused by excessive volume and dead space. The chapters that follow focus on general considerations in column attachment, measurement of column efficiency, and retention behavior of carrier gas, along with the operating temperature of the column, the choice of carrier gas, and carrier gas velocity. This book also looks at the factors that affect column stability, materials of restricted volatility, and some applications of glass capillary gas chromatography. This reference material is intended primarily for students and researchers interested in gas chromatography with glass capillary columns.

Gas Chromatography with Glass Capillary Columns describes glass capillary technology and the selection, installation, evaluation, and use of glass open tubular columns for gas chromatography. Discussions are organized around the glass capillary column; column coating and installation; inlet systems; measurement of column efficiency; temperature programming and carrier flow; and retention behavior. Column selection and stability and sample preparation are also covered. This text is comprised of 13 chapters; the first of which introduces the reader to the practical considerations involved in the selection, installation, evaluation, and use of high-resolution open tubular glass capillary columns, along with the theory of the chromatographic process. The discussion then turns to the influence of operating parameters and storage conditions on the interrelated forces involved in coating glass capillary columns; the dynamic and static techniques of column coating; and design defects in the inlet system caused by excessive volume and dead space. The chapters that follow focus on general considerations in column attachment, measurement of column efficiency, and retention behavior of carrier gas, along with the operating temperature of the column, the choice of carrier gas, and carrier gas velocity. This book also looks at the factors that affect column stability, materials of restricted volatility, and some applications of glass capillary gas chromatography. This reference material is intended primarily for students and researchers interested in gas chromatography with glass capillary columns.

Details

ISBN

978-0-12-384350-0

Language

English

Published

1978

Copyright

Copyright © 1978 Elsevier Inc. All rights reserved.

Imprint

Academic Press

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Authors

WALTER JENNINGS

Department of Food Science and Technology, University of California, Davis, California