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Table of contents
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CHAPTER 1 - INTRODUCTION
Pages 1-18 - Book chapterNo access
CHAPTER 2 - THE GLASS CAPILLARY COLUMN
Pages 19-29 - Book chapterNo access
CHAPTER 3 - COLUMN COATING
Pages 31-42 - Book chapterNo access
CHAPTER 4 - Inlet Systems
Pages 43-54 - Book chapterNo access
CHAPTER 5 - COLUMN INSTALLATION
Pages 55-66 - Book chapterNo access
CHAPTER 6 - MEASURING COLUMN EFFICIENCY
Pages 67-74 - Book chapterNo access
CHAPTER 7 - TREATMENT OF RETENTION DATA
Pages 75-82 - Book chapterNo access
CHAPTER 8 - TEMPERATURE PROGRAMMING AND CARRIER FLOW CONSIDERATIONS
Pages 83-91 - Book chapterNo access
CHAPTER 9 - COLUMN STABILITY
Pages 93-98 - Book chapterNo access
CHAPTER 10 - COLUMN SELECTION
Pages 99-104 - Book chapterNo access
CHAPTER 11 - SAMPLE PREPARATION
Pages 105-118 - Book chapterNo access
CHAPTER 12 - ANALYSIS OF MATERIALS OF RESTRICTED VOLATILITY
Pages 119-122 - Book chapterNo access
CHAPTER 13 - APPLICATIONS OF GLASS CAPILLARY GAS CHROMATOGRAPHY
Pages 123-146 - Book chapterNo access
APPENDIX I - NOMENCLATURE
Pages 147-152 - Book chapterNo access
APPENDIX II - LIQUID PHASES
Pages 153-158 - Book chapterNo access
APPENDIX III - POROUS POLYMER DATA
Pages 159-171 - Book chapterNo access
APPENDIX IV - SILYLATION AND DERIVATIZATION REACTIONS
Pages 173-179 - Book chapterNo access
INDEX
Pages 181-184
About the book
Description
Gas Chromatography with Glass Capillary Columns describes glass capillary technology and the selection, installation, evaluation, and use of glass open tubular columns for gas chromatography. Discussions are organized around the glass capillary column; column coating and installation; inlet systems; measurement of column efficiency; temperature programming and carrier flow; and retention behavior. Column selection and stability and sample preparation are also covered. This text is comprised of 13 chapters; the first of which introduces the reader to the practical considerations involved in the selection, installation, evaluation, and use of high-resolution open tubular glass capillary columns, along with the theory of the chromatographic process. The discussion then turns to the influence of operating parameters and storage conditions on the interrelated forces involved in coating glass capillary columns; the dynamic and static techniques of column coating; and design defects in the inlet system caused by excessive volume and dead space. The chapters that follow focus on general considerations in column attachment, measurement of column efficiency, and retention behavior of carrier gas, along with the operating temperature of the column, the choice of carrier gas, and carrier gas velocity. This book also looks at the factors that affect column stability, materials of restricted volatility, and some applications of glass capillary gas chromatography. This reference material is intended primarily for students and researchers interested in gas chromatography with glass capillary columns.
Gas Chromatography with Glass Capillary Columns describes glass capillary technology and the selection, installation, evaluation, and use of glass open tubular columns for gas chromatography. Discussions are organized around the glass capillary column; column coating and installation; inlet systems; measurement of column efficiency; temperature programming and carrier flow; and retention behavior. Column selection and stability and sample preparation are also covered. This text is comprised of 13 chapters; the first of which introduces the reader to the practical considerations involved in the selection, installation, evaluation, and use of high-resolution open tubular glass capillary columns, along with the theory of the chromatographic process. The discussion then turns to the influence of operating parameters and storage conditions on the interrelated forces involved in coating glass capillary columns; the dynamic and static techniques of column coating; and design defects in the inlet system caused by excessive volume and dead space. The chapters that follow focus on general considerations in column attachment, measurement of column efficiency, and retention behavior of carrier gas, along with the operating temperature of the column, the choice of carrier gas, and carrier gas velocity. This book also looks at the factors that affect column stability, materials of restricted volatility, and some applications of glass capillary gas chromatography. This reference material is intended primarily for students and researchers interested in gas chromatography with glass capillary columns.
Details
ISBN
978-0-12-384350-0
Language
English
Published
1978
Copyright
Copyright © 1978 Elsevier Inc. All rights reserved.
Imprint
Academic Press